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This paper studies the preparation of perillartine and N-tert-butyl-α-phenylnitrone (PBN) by vibrating and planetary ball-milling.
This webinar introduces the basic concepts of mechanochemistry, providing an overview of different reactor/milling techniques with a strong focus on scalable technologies.
This thesis endeavours to gain insight into the local kinetics from macroscopic experimental evidence in mechanochemical reactions.
A webinar session about ball mills and how to use them to scale up mechanochemical transformations.
This work studies the dynamics of single balls inside the jars of the most common oscillating ball mills.
Author(s): Dominik Lungerich, Clément Cabanetos, Jongseong Park, Sol Lee and Orein F. Jafter.
A general calculation method for traversing synthetic protocols derived from mixer or planetary ball mills; finding the point impact energy Eimpact of a single collision between the ball and the molecules, and the cumulative energy Etotal, which is transferred to the reaction mixture during the whole milling process.
Author(s): Evelina Colacino, Gandrath Dayaker, Alain Morère and Tomislav Friščić.
This education article describes a solvent-free mechanochemical synthesis in an undergraduate chemistry teaching laboratory. As a model reaction, the experiment addresses the catalytic mechanochemical synthesis of a small library of sulfonylureas, including a known active pharmaceutical ingredient, tolbutamide.